PDS_VERSION_ID = PDS3 LABEL_REVISION_NOTE = "2006-02-15, initial 2006-04-11, GEO:jgw, edited" RECORD_TYPE = STREAM OBJECT = INSTRUMENT INSTRUMENT_HOST_ID = RELAB INSTRUMENT_ID = NIC740_RELAB OBJECT = INSTRUMENT_INFORMATION INSTRUMENT_NAME = "RELAB NICOLET 740 FOURIER TRANSFORM INFRARED SPECTROMETER" INSTRUMENT_TYPE = "SPECTROMETER" INSTRUMENT_DESC = " Instrument Overview =================== Operating Spectral Range: Nominal (1.0 to 25 micrometers); Possible (0.75 to 25 micrometers) Mode Range (micrometer) Light Source Beam Splitter Detector ---- ------------------ ------------ ------------- -------- A 0.75-1.1 Quartz Quartz Silicon B 1.0-3.5 Quartz Quartz PbSe C 1.5-5.0 Glowbar KBr PbSe D 1.8-25.0 Glowbar KBr DTGS E 1.8-25.0 Glowbar KBr MCT (cooled) Sampling Interval: 16, 8, 4, 3, 1 or 0.5 cm**-1 Default: 8 cm**-1 (0.9-3.2 micrometers), 4 cm**-1 (1.8-26 micrometers) Geometry: Biconical - on axis for multiple sample holder Biconical - off axis for single measurement (and environment chamber) Transmission (normal incidence) Sample: Particulate sample or soil (reflectance): Measured horizontal and uncovered. Typical amount required is 500 mg. Sample should be no smaller than 20 mg. No more than 1 g is necessary in any case. Chip (reflectance): Measured horizontal and uncovered. Regions to be measured should be no smaller than 1 mm. Maximum sample size is 1 cm in diameter. Thin section and single crystal (transmission): Measured vertical, attached to an appropriate aperture board. Regions to be measured should be no smaller than 1.5 mm. Surface should be polished and clean (no carbon coating). Reference Standard: Brushed gold (reflectance) Blank (transmittance) FT-IR Spectromter: The Nicolet 740 is operational for samples of powders and small chips (<1 cm). Infrared biconical reflectance spectra are produced relative to a gold standard. Infrared spectra are typically scaled to and merged with bidirectional reflectance spectra to produce continuous spectra from 0.3 to 26 m. An environment chamber is operational with the Nicolet (10-3 Torr to 2 atmospheres; mixtures of up to 4 gases; temperatures 200-400 K). Use of the environment chamber requires user training and on-site operation. Please see [BISHOPETAL1995] for additional information. " END_OBJECT = INSTRUMENT_INFORMATION OBJECT = INSTRUMENT_REFERENCE_INFO REFERENCE_KEY_ID = "BISHOPETAL1995" END_OBJECT = INSTRUMENT_REFERENCE_INFO END_OBJECT = INSTRUMENT END